N-[(E)-4-(Methylsulfonyl)benzylidene]-3-nitroaniline

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(E)-N′-[(E)-3-(4-Hydr­oxy-3-methoxy­phen­yl)allyl­idene]isonicotinohydrazide

In the title compound, C(16)H(15)N(3)O(3), the dihedral angle between the pyridine and benzene rings is 7.66 (5)°. The crystal packing is consolidated by inter-molecular C-H⋯O and O-H⋯N inter-actions, which link the mol-ecules into zigzag chains propagating along [010]. The chains are further linked into a three-dimensional network by N-H⋯O, C-H⋯N, C-H⋯O and C-H⋯π inter-actions.

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N′-[(E)-4-Hydr­oxy-3-methoxy­benzyl­idene]benzohydrazide

In the title compound, C(15)H(14)N(2)O(3), the phenyl ring is disordered over two set of sites with an occupancy ratio of 0.810 (3):0.190 (3); the dihedral angle between the two components is 72.3 (4)°. The benzene and phenyl rings are oriented at dihedral angles of 69.18 (8) and 26.0 (5)° (major and minor orientations, respectively), and an intra-molecular O-H⋯O hydrogen bond occurs. In the cr...

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(E)-N′-(3-Benz­yloxy-4-methoxy­benzyl­idene)isonicotinohydrazide

In the title compound, C(21)H(19)N(3)O(3), the pyridine ring forms a dihedral angle of 15.25 (6)° with the benzene ring. The dihedral angle between the two benzene rings is 83.66 (7)°. The meth-oxy group is slightly twisted away from the attached ring [C-O-C-C = 7.5 (2)°]. In the crystal structure, mol-ecules are linked into a three-dimensional network by inter-molecular N-H⋯N and C-H⋯O hydroge...

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(E)-4-Amino-N′-(3-nitro­benzyl­idene)benzohydrazide

In the title compound, C(14)H(12)N(4)O(3), the dihedral angle between the benzene rings is 7.6 (4)°. In the crystal, infinite sheets linked by N-H⋯O and bifurcated N-H⋯(O,N) hydrogen bonds propagate in the (10-1) plane, in which R(4) (4)(36) loops are apparent. Neighbouring layers may inter-act by way of very weak π-π stacking inter-actions [centroid-centroid distances = 3.9329 (13) and 4.0702 ...

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4-Nitro-N′-[(E)-3-pyridylmethyl­idene]benzohydrazide

In the title moleclue, C(13)H(10)N(4)O(3), the methyl-idene-hydrazide [-C(=O)-N-N=C-] fragment is essentially planar, with a maximum deviation of 0.0228 (7) Å. The mean planes of the benzene and pyridine rings make dihedral angles of 25.44 (6) and 5.47 (7)°, respectively, with the mean plane of the methyl-idene-hydrazide fragment. In the crystal structure, inter-molecular N-H⋯N hydrogen bonds l...

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ژورنال

عنوان ژورنال: Acta Crystallographica Section E Structure Reports Online

سال: 2011

ISSN: 1600-5368

DOI: 10.1107/s1600536811031539